Read e-book online Actinide Separations PDF

By James D. Navratil and Wallace W. Schulz (Eds.)

ISBN-10: 0841205272

ISBN-13: 9780841205277

ISBN-10: 0841206821

ISBN-13: 9780841206823

content material: Neptunium (V) anionic alternate in sulfate-sulfuric acid ideas / J. Rego, J. Garrison, and R. Carver --
restoration of plutonium strains from nitric acid-fluorhydric acid suggestions by way of sorption onto alumina / J. Adroaldo De Araújo and Alcídio Abrão --
program of inorganic sorbents in actinide separations techniques / Wallace W. Schulz, John W. Koenst, and David R. Tallant --
Transplutonium components creation software : extraction chromatographic procedure for plutonium irradiated pursuits / J. Bourges, C. Madic, and G. Koehly --
Plutonium peroxide precipitation : overview and present learn / P.G. Hagan and F.J. Miner --
Actinide extractants : improvement, comparability, and destiny / R.R. Shoun and W.J. McDowell --
Demonstration of the potential of designing extractants with preselected extraction homes : attainable program to reactor gasoline reprocessing / G.W. Mason and H.E. Griffin --
Solvent extraction of transplutonium parts from acid ideas via polydentate impartial organophosphorus compounds and from alkaline ideas by means of quarternary ammonium bases and through alkylpyrocatechols / B.F. Myasoedov, M.K. Chmutova, and Z.K. Karalova --
The extraction of uranium (VI) from sulphuric acid strategies by means of tri-n-octylphosphine oxide / Taichi Sato --
homes and makes use of of nitrogen and sulfur donors ligands in actinide separations / C. Musikas, G. Le Marois, R. Fitoussi, and C. Cuillerdier --
The "Cleanex" strategy : a flexible solvent extraction approach for restoration and purification of lanthanides, americium, and curium / John E. Bigelow, Emory D. Collins, and Lester J. King --
Americium-curium separation via selective extraction of hexavalent americium utilizing a centrifugal contactor / C. Musikas, M. Germain, and A. Bathellier --
nationwide application for pyrochemical and dry processing of spent reactor gasoline / C.H. Bean and M.J. Steindler --
Pyrochemical coprocessing of uranium dioxide-plutonium dioxide LMFBR gas via the salt shipping procedure / James B. Knighton and Charles E. Baldwin --
A nonaqueous reprocessing process for thorium-based fuels / J.K. Bates, L.J. Jardine, and M. Krumpelt --
AIROX dry pyrochemical processing of oxide fuels : a proliferation-resistant reprocessing technique / L.F. Grantham, R.G. Clark, R.C. Hoyt, and J.R. Miller --
Molten salt oxidation-reduction methods for gas processing / L.G. Morgan, L.L. Burger, and R.D. Scheele --
Photochemistry of the actinides / L.M. Toth, J.T. Bell, and H.A. Friedman --
program of photochemical innovations to actinide separation strategies / G.L. Depoorter and C.K. Rofer-Depoorter --
Plutonium partitioning tools in strength reactor gas reprocessing / Alfred Schneider and Barry G. Wahlig --
improvement of the electropulse column for uranium-plutonium partition within the AGNS reprocessing plant / A.F. Cermak and R.G. Spaunburgh --
Electroredox tactics for plutonium in strength reactor gas reprocessing / Franz Baumgärtner, Hubert Goldacker, and Helmut Schmieder --
The separation of uranium and plutonium by way of electrolytic relief within the purex technique / He Jian-Yu, Zhang Qing-Xuan, and Lo Long-Jun --
experiences on actinides separation in JAERI / Tomitaro Ishimori --
Heavy aspect separation for thorium-uranium-plutonium fuels / G.R. provide, W.W. Morgan, K.K. Mehta, and F.P. Sargent --
advancements in thorium-uranium separation within the acid-thorex strategy / Glen E. Benedict --
Actinide partitioning flowsheets / D.D. Tedder, B.C. Finney, and J.O. Blomeke --
Flowsheet improvement paintings on the Idaho Chemical Processing Plant for the partitioning of actinides from acidic nuclear waste / L.D. McIsaac, J.D. Baker, J.F. Krupa, D.H. Meikrantz, and N.C. Schroeder --
restoration of spinoff actinides from energy reactor fuels and creation of warmth resource isotopes / G. Koch --
Separation of actinides from purex-type excessive lively waste raffinates : improvement of experimental stories at JRC-ISPRA institution / L. Cecille, H. Dworschak, F. Girardi, B.A. Hunt, F. Mannone, and F. Mousty --
elimination of americium and curium from high-level wastes / W.D. Bond and R.E. Leuze --
Americium restoration and purification at Rocky residences / James D. Navratil, Larry L. Martella, and Gary H. Thompson --
The extraction of DBP and MBP from actinides : software to the restoration of actinides from TBP-sodium carbonate scrub answer / E.P. Horwitz, G.W. Mason, C.A.A. Bloomquist, R.A. Leonard, and G.J. Bernstein --
Dissolution of plutonium dioxide : a serious assessment / Jack L. Ryan and Lane A. Bray --
fresh Savannah River adventure and improvement with actinide separations / M.C. Thompson, G.A. Burney, and J.M. McKibben --
Separation of long-lived [alpha]-emitters from hugely radioactive ideas within the thorium-uranium gasoline cycle / U. Wenzel, C.L. Branquinho, D. Herz, and G. Ritter --
Laboratory and pilot plant reviews on conversion of uranyl nitrate to uranium hexafluoride / I.J. Urza and D.C. Kilian --
Separation of actinides from excessive energetic waste via counter present ion migration / B.A. Bilal, F. Herrmann, okay. Metscher, B. Mühlig, Ch. Reichmuth, and B. Schwarz --
Polymolybdates as plutonium (IV) hosts / R.A. Penneman, R.G. Haire, and M.H. Lloyd.

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D e s t r u c t i o n o f s t a t i o n a r y p h a s e : b l a c k e n i n g and p a r t i a l c o l l a p s e o f t h e b e d . P a r t i a l c l o g g i n g o f c o l u m n s b y f o u l i n g ( i n s o l u b l e f i s s i o n p r o d u c t s ? ) . Drop i n e x c h a n g e capacity _ 1 o f the column a s s o c i a t e d w i t h o b s e r v a t i o n s 1 and 2. A l l t h e s e o c c u r e n c e s r e q u i r e replacement o f t h e columns e v e r y 3 o r 4 c y c l e s . I n M . A . o r L . A .

Q p r e v i o u s l y t r e a t e d b y t h e o x i d i z i n g s o l u ­ t i o n u n t i l maintenance o f the A g c o l o r a t i o n i n the e f f l u e n t s o l u t i o n . Americium i n o x i d a t i o n s t a t e VI i s f i x e d , g i v i n g a r i n g o f a g r e e n i s h c o l o r . The c o l u m n i s t h e n s c r u b b e d w i t h t h e o x i d i ­ z i n g s o l u t i o n . The a m e r i c i u m i s e l u t e d b y a s o l u t i o n o f c o m p o s i ­ 2 + t i o n : CN2H5N03= 0 . 5 M , CHN03 = 1M.

The two TBP c o l u m n s mounted i n s e r i e s h a v e an e x c h a n g e c a p a ­ c i t y o f 110 g o f l a n t h a n i d e s (mean a t o m i c w e i g h t 150 g ) , a l l o w i n g the f i x a t i o n o f the l a n t h a n i d e s p r e s e n t i n a h a l f t a r g e t . T h i s b e h a v i o u r i s c e r t a i n l y n o t o b t a i n e d and i t may be e s t i m a t e d t h a t a l a r g e f r a c t i o n o f l i g h t elements e s c a p e s i n t h e f i x a t i o n s t a g e . I n a c t u a l f a c t , a s i n g l e p a i r o f columns i s s u f f i c i e n t f o r the second p u r i f i c a t i o n c y c l e , w h i c h g r o u p s a l l t h e a m e r i c i u m and c u r i u m p r e ­ sent i n t h e t a r g e t .

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Actinide Separations by James D. Navratil and Wallace W. Schulz (Eds.)

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